Class Summary          12/01/04         

 

12/01               Cope Rearrangment

 

            What is the mechanism of the Cope Rearrangement?

                        NOT IONIC

                        Proposed intermediate is a six-membered transition state

                        Structure can be either a cyclohexyl-like system, or a biallyl system

Analysis of the products suggest that the intermediate is a chair-like cyclohexyl species (Doering, 1962)

 

Substituents play an important role in the nature of the Cope transition state

(Kinetics, energetics, product analysis were used to divine details)

 

            What is the nature of the Cope transition state?

                        Variable transition state for Cope (varies between biradical cyclohexyl and diallyl system)

                        Gajewski used deuterated species and studied kinetics of bond-breaking and bond-making.

           

 

RELEVANT REFERENCES

 

Cope, A.C. and Hardy, E.M.  The Introduction of Substituted Vinyl Groups. V. A Rearrangement Involving the Migration of an Allyl Group in a Three-Carbon System  J. Am. Chem. Soc. (1940) 62, 441-444.

Levy, H. and Cope, A.C.  The Rearrangement of Allyl Groups in Three-carbon Systems. IV. Hydrocarbons  J. Am. Chem. Soc. (1944) 66, 1684-1688.

 

Doering, W. von E. and Roth , W.R.  The overlap of two allyl radicals or a four-centered transition state in the cope rearrangement  Tetrahedron (1962) 18, 67-74.

 

Gajewski, J.J. and Conrad, N.D.  Variable transition state structure in 3,3-sigmatropic shifts from a-secondary deuterium isotope effects  J. Am. Chem. Soc. (1979) 101, 6693-6704.



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